ANALYTICAL CHEMISTRY
II LAB |
HOME | SYLLABUS | COURSE DESCRIPTION | LAB MANUAL | COURSE SCHEDULE | RYAN RESEARCH GROUP |
Lab Manual Must Be Downloaded or Printed by Students From the Link Given Above
Week |
Experiment |
Course Material |
1 | Lab Orientation/Safety | |
2-4 | Determination of Caffeine and Acetylsalicylic Acid in an Analgesic Tablet by Ultraviolet Spectrophotometry Determination of the Active Ingredient in a Pharmaceutical Preparation by Fluorometry FT-IR: Comparison of Sample Preparation Techniques and Interpretation of Spectra of Unknown |
Caffeine & ASA by UV-vis (wmv) Active Ingredient by Fluorometry (wmv) Sample Prep & Unknown by FT-IR (wmv) |
5-7
|
Flame Atomic Absorption (AA) of Metals in Pet Food Sample and Comparision with DC Plasma Determination of Cu, Na, Zn, Mn and Fe in Pet Food by Direct Current Plasma Atomic Emission Spectroscopy Determination of Cu Concentration in Waters by Graphite Furnace Atomic Spectroscopy |
Flame AA (video) Pet Food by DCP (wmv) Copper in Water by GFAA (wmv) |
8-10 |
Gas Chromatography: Separation of Organic Compounds Determination of Food Additives by High Performance Liquid Chromatography (HPLC): Caffeine in Beverages Determination of Metal Ions in Drinking Water by Square Wave Voltammetry (SWV) |
Organic Separation by GC(wmv) Caffeine in Beverages by HPLC (wmv) Square Wave Voltammetry (SWV) (video) |
11-13 |
Determination of Chloride using Ion-Selective Electrode (ISE) Identification of Organics in an Unknown Mixture: an experiment by FT-IR and GC-MS Spectrophotometric Determination of Formula and Stability Constant of Complex Ions |
Chloride in Water by Chloride ISE (wmv) Fragrances Identification by GC-MS (wmv) Stability Constant by UV-vis (wmv) |
14 | Lab Cleanup |
© 2005 University of Massachusetts Lowell |